[1]窦天全①,曾光伟①,李学平①,等.无粉尘球状DDNP球形化工艺研究[J].爆破器材,2012,41(06):30-33.[doi:10.3969/J.ISSN.1001-8532.2012.06.009]
DOU Tianquan,ZENG Guangwei,LI Xueping,et al.Spheroidization Technology Study of Dustless Spheroidal DDNP[J].EXPLOSIVE MATERIALS,2012,41(06):30-33.[doi:10.3969/J.ISSN.1001-8532.2012.06.009]
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无粉尘球状DDNP球形化工艺研究()
《爆破器材》[ISSN:1001-8352/CN:32-1163/TJ]
- 卷:
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41
- 期数:
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2012年06
- 页码:
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30-33
- 栏目:
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爆破技术
- 出版日期:
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2012-12-20
文章信息/Info
- Title:
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Spheroidization Technology Study of Dustless Spheroidal DDNP
- 文章编号:
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4494
- 作者:
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窦天全①; 曾光伟①; 李学平①; 钟攀①; 高欣②; 刘效标③
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①雅化集团绵阳实业有限公司(四川绵阳,621107)
②雅化集团股份公司(四川雅安,625000)
③长沙绿光环保技术开发有限公司(湖南长沙,410000)
- Author(s):
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DOU Tianquan①; ZENG Guangwei①; LI Xueping①; ZHONG Pan①; GAO Xin②; LIU Xiaobiao③
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①Mianyang Industrial Co.,Ltd. of Sichuan Yahua Group ( Sichuan Mianyang,621107)
②Sichuan Yahua Industrial Group Co., Ltd. (Sichuan Ya’an,625000)
③Changsha Lvguang Environmental Technology Development Co., Ltd. (Hu’nan Changsha, 410000)
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- 关键词:
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无粉尘; 球状; DDNP
- Keywords:
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without dust; spheroidal; DDNP
- 分类号:
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TQ563 TD235.2+2
- DOI:
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10.3969/J.ISSN.1001-8532.2012.06.009
- 文献标志码:
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A
- 摘要:
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文章研究了无粉尘球状DDNP工艺的还原和重氮。还原采用硫化钠直接还原苦味酸,加上特殊的控制结晶技术使生产的氨基苦味酸钠颗粒均匀;重氮采用加入连苯三酚作为晶型控制剂,X1作为晶型引导剂,使DDNP成球状,无粉尘。文章还试验研究了球状DDNP的特性。与传统工艺相比,新工艺生产的球状DDNP的极限药量为60 mg,略高于传统工艺;耐压性能在53 MPa以上,略高于传统工艺;撞击感度、摩擦感度低于传统工艺;静电火花感度与传统工艺相当。
- Abstract:
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The reduction and diazotization of dustless spheroidal DDNP were studied in this paper. Sodium sulfide is used to reduce picric acid to achieve even granules of amino sodium picrate under controlled crystallization. Pyrogallol is introduced as crystal controller together with X1 as crystal inducer during dizzotization to spherize DDNP without dust. In comparison with conventional technology, the performance of spheroidal DDNP was evaluated as slightly increased limiting charge of 60 mg, pressureresistant of above 53 MPa, lower impact sensitivity and friction sensitivity, and equivalent electrostatic spark sensitivity.
参考文献/References:
[1]劳允亮.起爆药化学与工艺学[M].北京:北京理工大学出版社,2004.
[2]蒋荣光,刘自铴.起爆药[M].北京:兵器工业出版社,2006.
[3]Evans R. N. Development of Composite Motor Technology for the Advanced Kinetic Energy Missile[R]//28th Joint Propulsion Conference and Exhibit. 1992.
[4]赵杰,郭俊国,刘建新,等.一种DDNP制造新技术[J].爆破器材,2008,37(1):29-30.
[5]劳允亮,盛涤沦.火工药剂学[M].北京:北京理工大学出版社,2011.
[6]刘登程,杨宗伟,刘玉存,等.球形DDNP制备技术研究[J].含能材料,2009,17(5):619-623.
[7]陈淮银,王代钧,梁立达.DDNP生产及其污水处理新工艺[J].爆破器材,1993,22(1):14-16.
[8]孙德强,李月明.对提高DDNP得率及控制产品质量因素的分析[J].爆破器材,2003,32(2):14-16.
备注/Memo
- 备注/Memo:
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收稿日期:2012-05-15
作者简介:窦天全(1985~),男,助理工程师,主要从事起爆器材研究。
通信作者:李学平(1974~),男,工程师,主要从事起爆器材研究制造。
更新日期/Last Update:
2012-12-31